نتایج جستجو برای: Solid state reaction
تعداد نتایج: 1378548 فیلتر نتایج به سال:
this work is presented in five parts. in the first part preparation of the starting complex [pt(c^n)cl(dmso)], 1, in which c^n = n(1),c(2?)-chelated, deprotonated 2-phenylpyridine, and dmso = dimethylsulfoxide, and its reaction with 1 equiv of the biphosphine ligands bis(diphenylphosphino)amine, dppa, or bis(diphenylphosphino)methane, dppm, to give the complex [pt(c^n)cl(dppa)], 2, or [pt(c^n)c...
a basic alumina-spinel low cement castable (lcc) composed of sintered bauxite, reactive alumina, calcined alumina, calcined magnesia, microsilica, and high alumina refractory cement was prepared (castable a) to which 5% sodium hexa-meta phosphate was later added (castable b) to prepare samples for heat treatment at 110ºc, 900ºc, and 1400ºc. bulk density (bd), apparent porosity (ap), and cold cr...
the nanopowders of sno2, casno3 and ca2sno4 in the size rang of 5-70 nm have been prepared using solid-state reaction technique. the technique is convenient and inexpensive in comparison to the conventional routes of compound prepared and processing where, many steps of mixing and annealing are involved. formation of resultant compounds was explained on the basis of reaction taken place between...
ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 complex was prepared according to literature report. the reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. the [ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (ni1-ni5) was ...
ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 complex was prepared according to literature report. the reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. the [ni6(n2h4)6(so4)4(oh)2(h2o)8](so4)(h2o)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (ni1-ni5) was ...
The synthesis of calcium tetraborate was investigated in a temperature ranging from 800℃ to 900℃ using the solid-state reaction method. The synthesis was done using ammonium tetraborate tetrahydrate as the source of boron. At temperatures of 800 ℃ and 880 ℃, the mixed phases from different compounds were formed. At the optimum temperature of 840℃, the mixed phase was only composed of meta and t...
Ni6(N2H4)6(SO4)4(OH)2(H2O)8](SO4)(H2O)10 complex was prepared according to literature report. The reaction between aforementioned complex via sodium alkoxides as a reactants, were carried out in the solid state. The [Ni6(N2H4)6(SO4)4(OH)2(H2O)8](SO4)(H2O)10 undergoes an intramolecular two electrons oxidation-reduction reaction at room temperature and metallic nickel nanoparticles (Ni1-Ni5) was ...
This paper describes the synthesis of Pb(Zr0.95Ti0.05)O3 powder by sol gel and solid state methods. PZT powders were fabricated by solid-state reaction process using metal oxides and in sol gel method salts and organic compounds were employed. The powders were calcined at 700 and 950 oC in sol gel and solid state methods, respectively. The synthesized powders were analyzed by FTIR and XRD. Th...
a simple extremely fast and efficient approach for the synthesis of substituted indazole ingood to excellent yield catalyzed by using silica sulfuric acid (ssa) in dmso solvent at roomtemperature. this is solid state reaction have been attracting the synthetic organic chemist asthey provided enhance reaction rates, less environmental pollution, greater selectivity, cleanerproducts and manipulat...
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